HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12461092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (Oxiran-2-yl)methyl methanesulfonate | HCID 110799 | — |
| Product | HCID 12461092 | HCID 12461092 | 85% |
Reaction Steps
Concentrated HCl (20 ml) was added to 3-mesyloxy-1,2-epoxypropane (5.0 g, 0.033 m) over 15-20 minutes. After stirring for an additional 30 minutes, the water was removed through the addition and subsequent evaporation of ethanol. Finally, residual ethanol was removed at room temperature and 0.1 mm to give 3-mesyloxy-2-hydroxy-1-chloropropane (5.4 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588824 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-09c6936c4bc24d39a6df3b5fb0066b2c |
| Source note | uspto-grants-1986_05 |