HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 2-(2'-Benzylthio-5'-chlorophenyl)-imidazolidine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 4-Chlorobenzothietane-2-spiro-2'-imidazoline | HCID 70469119 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(2'-Benzylthio-5'-chlorophenyl)-imidazolidine hydrochloride | HCID 23320419 | — |
Reaction Steps
32 parts of 4-chlorobenzothietane-2spiro-2'-imidazolidine is reacted with 19 parts of benzyl chloride in 300 parts of methanol as described in Example 11. The yield is 43 parts (84% of theory) and the melting point is 260° C. with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE032154 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-3d368d9093da4335bf537a9da68c0272 |
| Source note | uspto-grants-1986_05 |