Thiirane, 2-methyl- → HCID 13049112, compound

HRID 280489Notes

Reaction equation

HRID 280489 reaction equation
[CH2:1]1[S:4][CH:2]1[CH3:3].[CH3:5][N:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH2:7]1>>[SH:4][CH:2]([CH3:3])[CH2:1][N:9]1[CH2:10][CH2:11][N:6]([CH3:5])[CH2:7][CH2:8]1

Participants

3

Reactant 2

HCID 14072Thiirane, 2-methyl-HCID 531671-Methylpiperazine

Product 1

HCID 13049112HCID 13049112, compound

Procedure

The 1-(2-mercaptopropyl)-4-methylpiperazine is prepared by heating a mixture of propylene sulphide (19 cc) and N-methylpiperazine (29 cc) at 100° C. for 16 hours. This gives a colourless oil (32 g) distilling at 105° C. under 1.3 kPa.

Workup

  1. temperatureby heating

Sources & evidence

ORD record
ord-647ca319a1c1436fb604072cd5bb19f0
Source dataset
uspto-grants-1986_05
Patent number
US04590004

Reaction notes

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