Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → Cycloheptyl-2-mercaptopropionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | Cycloheptanol | HCID 10399 | — |
| 반응물 | (+-)-2-Mercaptopropionic acid | HCID 62326 | — |
| 생성물 | Cycloheptyl-2-mercaptopropionate | HCID 20212360 | — |
반응 단계
Reaction: ##STR128## Into a 50 ml reaction flask equipped with stirrer, thermometer, reflux condenser and heating mantle are placed 11.4 grams cycloheptanol; 22 grams of 2-mercaptopropionic acid and 0.5 grams of paratoluene sulfonic acid. The reaction mass is heated to reflux and refluxed for a period of 10 hours. At the end of the 10 hour period, the reaction mass is distilled on a micro distillation apparatus to yield the compound having the structure: ##STR129##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04590082 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-7865c488157c425f9ced1af031fe9972 |
| 출처 메모 | uspto-grants-1986_05 |