5-((Dimethylamino)methyl)-2-furanmethanol → HCID 70515975, compound

Participants

Reaction Steps

To a stirred solution of N3 -[2-mercapto ethyl]-1,2-benzoisothiazole-3,4-diamine-1,1-dioxide (D.9, 0.11 g) in concentrated hydrochloric acid (0.4 ml) under nitrogen at -10° C. was added 5-dimethylaminomethyl-2-furanmethanol (0.08 g). After stirring at room temperature overnight, the reaction mixture was worked-up as described in Example 2 to afford the title compound.

Provenance & Evidence