HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13376232, compound → Methyl 5-(2-chloroethoxy)thiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13376232 | HCID 13376232 | — |
| Reactant | HCID 13376233 | HCID 13376233 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | Methyl 5-(2-chloroethoxy)thiophene-2-carboxylate | HCID 13376214 | — |
Reaction Steps
3-Methyl-5-(2-chloro-1-ethoxy)-thiophene-2-carboxylic acid methyl ester, melting point (MeOH/H2O) 47°-50° C. (86%), and 4-Methyl-5-(2-chloro-1-ethoxy)-thiophene-2-carboxylic acid methyl ester, melting point (petroleum ether) 75° C. (90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04590203 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-21a809119f2244478caf18869078af01 |
| Source note | uspto-grants-1986_05 |