HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → 7-Bromo-2-dimethylaminomethyl-1-tetralone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 7-Bromo-2-dimethylaminomethyl-1-tetralone hydrochloride | HCID 23320933 | — |
| Solvent | Water | HCID 962 | — |
| Product | 7-Bromo-2-dimethylaminomethyl-1-tetralone | HCID 13663057 | — |
Reaction Steps
The hydrochloride was converted to the free base by dissolving in a small volume of water and adding a slight excess of a saturated aqueous solution of sodium bicarbonate. Ether extraction gave the free base as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04590200 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-db0c8c3ecc994e628a5282a8005ae732 |
| Source note | uspto-grants-1986_05 |