HRID280877

反应详情

EQUATION

反应方程式

HRID 280877 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

27 g of 3',4'-dibenzyloxy-5,7-dihydroxy-3-cyclohexyloxyflavone, 500 cc of acetone, 500 cc of methyl alcohol, 8 spatulas of palladium on 5% BaSO4 are introduced in a 2-liter round-bottom flask. The mixture is stirred under an hydrogen atmosphere for 3 hours. The reaction is followed with thin-layer chromatography. After filtering on millipores, the solution is evaporated. Yield 98%.

WORKUP

后处理

  1. filtrationAfter filtering on millipores
  2. customthe solution is evaporated