HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 13370458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Barium Sulfate | HCID 24414 | — |
| Reactant | HCID 23320230 | HCID 23320230 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13370458 | HCID 13370458 | 98% |
Reaction Steps
27 g of 3',4'-dibenzyloxy-5,7-dihydroxy-3-cyclohexyloxyflavone, 500 cc of acetone, 500 cc of methyl alcohol, 8 spatulas of palladium on 5% BaSO4 are introduced in a 2-liter round-bottom flask. The mixture is stirred under an hydrogen atmosphere for 3 hours. The reaction is followed with thin-layer chromatography. After filtering on millipores, the solution is evaporated. Yield 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04591600 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-22d5e911ea6e4b08aaffa7d6127caf4f |
| Source note | uspto-grants-1986_05 |