Hydrochloric Acid → HCID 18936298, compound

HRID 2821Notes

Reaction equation

HRID 2821 reaction equation
[CH3:1][C:2]1[O:3][C:4]([C:8]([C:12]2[CH:16]=[CH:15][O:14][CH:13]=2)(OC)[CH3:9])=[C:5]([CH3:7])[N:6]=1.[ClH:17]>C(OCC)C>[ClH:17].[CH3:1][C:2]1[O:3][C:4]([C:8]([C:12]2[CH:16]=[CH:15][O:14][CH:13]=2)=[CH2:9])=[C:5]([CH3:7])[N:6]=1

Participants

4

Procedure

1-(2,4-Dimethyl-5-oxazolyl)-1-(3-furyl)-1-methoxyethane (790 mg) in dry diethylether was treated with 1M anhydrous hydrogen chloride in diethylether (1.2 equivalents). The title compound was obtained as a white solid which was filtered off, washed and dried. M.p. 128.5°-130° C.

Sources & evidence

ORD record
ord-9563069ad89e455ea5d20776f1f48877
Source dataset
uspto-grants-1998_03
Patent number
US05731335

Reaction notes

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