HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 23339566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Ethyl 4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate | HCID 12866705 | — |
| Reactant | HCID 23339577 | HCID 23339577 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 23339566 | HCID 23339566 | — |
Reaction Steps
This compound is prepared by the method described in Example 4, Step B, except that an equivalent quantity of ethyl 2-chloro-4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate is substituted for the ethyl 4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate of Example 4, Step B. The title compound is obtained as an oil by column chromatography on silica gel with 2% methanol in chloroform as eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04225609 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-1313e4612f0644a38a4617d65665a7c9 |
| Source note | uspto-grants-1980_09 |