HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18936306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 18936311 | HCID 18936311 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18936306 | HCID 18936306 | — |
Reaction Steps
1-(3-Furyl)-1-(2,4-dimethyl-5-oxazolyl)ethanol (2g) in dry N,N-dimethylformamide (15 ml) was added to a stirred suspension of sodium hydride (80%, 300 mg) in dry N,N-dimethylformamide (10 ml) at 0° C. After 20 minutes, methyl iodide (1.5 g) was added dropwise. The mixture was allowed to warm to room temperature and after 30 minutes aqueous sodium hydrogen carbonate was added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731335 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-59fd6eb77b07405893186404a2c88e70 |
| Source note | uspto-grants-1998_03 |