HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 59788256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | 4-Chloro-6-(2,3-dichlorophenyl)pyrimidin-2-amine | HCID 87645982 | — |
| Product | HCID 59788256 | HCID 59788256 | 42% |
Reaction Steps
Following the method described in Example 53, 4-chloro-6-(2,3-dichloro-phenyl)-pyrimidin-2-ylamine and 4-chloroaniline provided the title compound (42% yield). 1H NMR (CD3OD) δ 6.19 (s, 1H, Ar), 7.29 (d, 2H, Ar), 7.31 (d, 2H, Ar) 7.4 (d, 1H, Ar) 7.55 (d, 2H, Ar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07419984B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-21cd60faad944deda9ddb59d9eb5b321 |
| Source note | uspto-grants-2008_09 |