Dimethylamine → HCID 68995145, compound

HRID 28972Notes

Reaction equation

HRID 28972 reaction equation
[Br:1][C:2]1[C:3]([C:8]2[CH:13]=[CH:12][C:11]([NH2:14])=[CH:10][CH:9]=2)=[N:4][N:5]([CH3:7])[CH:6]=1.[CH3:15][NH:16][CH3:17].[O:18]1[CH2:22]CCC1>>[Br:1][C:2]1[C:3]([C:8]2[CH:13]=[CH:12][C:11]([NH:14][C:22](=[O:18])[N:16]([CH3:17])[CH3:15])=[CH:10][CH:9]=2)=[N:4][N:5]([CH3:7])[CH:6]=1

Participants

4

Reactant 3

HCID 674DimethylamineHCID 8028TetrahydrofuranHCID 27353923-(4-Aminophenyl)-4-bromo-1-methylpyrazole

Product 1

HCID 68995145HCID 68995145, compound

Procedure

Following the procedure described for Example 5a using [4-(4-bromo-1-methyl-1H-pyrazol-3-yl)phenyl]amine and 2M dimethylamine in tetrahydrofuran provided the title compound. ESMS [M+H]+: 323.2

Sources & evidence

ORD record
ord-c7a1e4f3000e47dab2a35ac5418177bf
Source dataset
uspto-grants-2008_09
Patent number
US07419988B2

Reaction notes

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