HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Ethyl 4-(1-methoxyethyl)-3-methyl-1-benzofuran-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 68714719 | HCID 68714719 | — |
| Product | Ethyl 4-(1-methoxyethyl)-3-methyl-1-benzofuran-2-carboxylate | HCID 68712409 | 100% |
Reaction Steps
According to the procedure of (Example 100, Step 1), 0.21 g of ethyl 4-(1-hydroxyethyl)-3-methyl-1-benzofuran-2-carboxylate after heating with iodomethane for 8 days provided 0.22 g of ethyl 4-(1-methoxyethyl)-3-methyl-1-benzofuran-2-carboxylate. Yield: ˜100% m.p. 67-69° C.; MS: 263.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07420001B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-8d2b1375a53045bba633db400b013e69 |
| Source note | uspto-grants-2008_09 |