Triethylamine → 4-nitro-N-(3-{[(4-nitrophenyl)amino]methyl}benzyl)aniline

Participants

Reaction Conditions

Reaction Steps

1.73 g of para-fluoronitrobenzene (2 eq.) were dissolved in 5 ml of DMSO. 1.2 equivalents of m-xylenediamine and 4 equivalents of triethylamine were added to the solution. The reaction mixture was heated at 60° C. for 20 hours. The mixture was then poured onto crushed ice and a precipitate formed. The latter was filtered, washed with water, and then dried.

Provenance & Evidence