反应详情

温度

60 °C

1.73 g of para-fluoronitrobenzene (2 eq.) were dissolved in 5 ml of DMSO. 1.2 equivalents of m-xylenediamine and 4 equivalents of triethylamine were added to the solution. The reaction mixture was heated at 60° C. for 20 hours. The mixture was then poured onto crushed ice and a precipitate formed. The latter was filtered, washed with water, and then dried.

1. additionThe mixture was then poured
2. customonto crushed ice
3. customa precipitate formed
4. filtrationThe latter was filtered
5. washwashed with water
6. customdried