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HRID29806

反应详情

EQUATION

反应方程式

HRID 29806 的结构方程式

REACTANTS

反应物

1
结构：COC(=O)c1cccc(C(=O)NNC(C)=N)c1
HCID178497871

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cccc(-c2n[nH]c(C)n2)c1
HCID69217670

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

8.10 g (34.4 mmol) methyl 3-[N′-(1-imino-ethyl)-hydrazinocarbonyl]-benzoate are heated to 180° C. for 30 minutes. 80 mL chloroform are added to the solid obtained after cooling. The suspension is filtered and the product is dried. White solid.

WORKUP

后处理

  1. customobtained
  2. temperatureafter cooling
  3. filtrationThe suspension is filtered
  4. customthe product is dried