HCID 178497871, compound → methyl 3-(5-methyl-1H-[1,2,4]triazol-3-yl)-benzoate

HRID 29806Notes

Reaction equation

HRID 29806 reaction equation
[NH:1]=[C:2]([NH:4][NH:5][C:6]([C:8]1[CH:9]=[C:10]([CH:15]=[CH:16][CH:17]=1)[C:11]([O:13][CH3:14])=[O:12])=O)[CH3:3]>C(Cl)(Cl)Cl>[CH3:3][C:2]1[NH:4][N:5]=[C:6]([C:8]2[CH:9]=[C:10]([CH:15]=[CH:16][CH:17]=2)[C:11]([O:13][CH3:14])=[O:12])[N:1]=1

Participants

3

Reactant 1

HCID 178497871HCID 178497871, compound

Product 1

HCID 69217670methyl 3-(5-methyl-1H-[1,2,4]triazol-3-yl)-benzoate

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

8.10 g (34.4 mmol) methyl 3-[N′-(1-imino-ethyl)-hydrazinocarbonyl]-benzoate are heated to 180° C. for 30 minutes. 80 mL chloroform are added to the solid obtained after cooling. The suspension is filtered and the product is dried. White solid.

Workup

  1. customobtained
  2. temperatureafter cooling
  3. filtrationThe suspension is filtered
  4. customthe product is dried

Sources & evidence

ORD record
ord-4c1cda77f3b54753bc080c7c186804f4
Source dataset
uspto-grants-2008_09
Patent number
US07423036B2

Reaction notes

Loading…