HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178497871, compound → methyl 3-(5-methyl-1H-[1,2,4]triazol-3-yl)-benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178497871 | HCID 178497871 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | methyl 3-(5-methyl-1H-[1,2,4]triazol-3-yl)-benzoate | HCID 69217670 | — |
Reaction Steps
8.10 g (34.4 mmol) methyl 3-[N′-(1-imino-ethyl)-hydrazinocarbonyl]-benzoate are heated to 180° C. for 30 minutes. 80 mL chloroform are added to the solid obtained after cooling. The suspension is filtered and the product is dried. White solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423036B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-4c1cda77f3b54753bc080c7c186804f4 |
| Source note | uspto-grants-2008_09 |