Phosphorus oxychloride → HCID 86612218, compound

HRID 29968Notes

Reaction equation

HRID 29968 reaction equation
[CH2:1]([C:8]1[C:17]2[C:12](=[CH:13][C:14]([O:20][CH3:21])=[CH:15][C:16]=2[O:18][CH3:19])[C:11](=O)[NH:10][N:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.P(Cl)(Cl)([Cl:25])=O>>[CH2:1]([C:8]1[C:17]2[C:12](=[CH:13][C:14]([O:20][CH3:21])=[CH:15][C:16]=2[O:18][CH3:19])[C:11]([Cl:25])=[N:10][N:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 69212999HCID 69212999, compound

Product 1

HCID 86612218HCID 86612218, compound

Procedure

This compound is obtained according to the procedure described in 1.3. by reacting 4-benzyl-5,7-dimethoxy-2H-phthalazin-1-one with phosphoryl chloride.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-e68bbe1c700b4cc1b2e39d03f1297cf6
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

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