Phosphorus oxychloride → HCID 86612224, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([C:7]([C:14]3[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][CH:15]=3)=[N:8][NH:9][C:10]2=O)=[CH:5][CH:4]=1.P(Cl)(Cl)([Cl:23])=O>>[Cl:23][C:10]1[C:11]2[C:6](=[CH:5][CH:4]=[C:3]([O:2][CH3:1])[CH:12]=2)[C:7]([C:14]2[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][CH:15]=2)=[N:8][N:9]=1Participants
3
Procedure
This compound is obtained according to the procedure described in 1.3. by reacting 7-methoxy-4-(4-methylphenyl)-2H-phthalazin-1-one with phosphoryl chloride.
Workup
- customThis compound is obtained
Sources & evidence
- ORD record
- ord-49c6508b711949a4b71440bdeb040ea7
- Source dataset
- uspto-grants-2008_09
- Patent number
- US07423030B2
Reaction notes
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