HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-5-methoxybenzoic acid → 5-Methoxy-2-(4-methoxymethylbenzoyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-5-methoxybenzoic acid | HCID 89906 | — |
| Reactant | n-Methoxy-4-methoxymethyl-n-methylbenzamide | HCID 60645894 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | 5-Methoxy-2-(4-methoxymethylbenzoyl)benzoic acid | HCID 69214250 | — |
Reaction Steps
This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-4-methoxymethyl-N-methylbenzamide. The product is crystallized from diisopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423030B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-a7452d63123c42d1972cb33cffe8ea84 |
| Source note | uspto-grants-2008_09 |