Hydrazine hydrate (1:1) → 4-(3,4-dimethylphenyl)-7-methoxy-2H-phthalazin-1-one

HRID 30039Notes

Reaction equation

HRID 30039 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[CH3:21])[C:5]([C:7]1[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][C:8]=1[C:9](O)=[O:10])=O.O.[NH2:23][NH2:24]>>[CH3:1][C:2]1[CH:3]=[C:4]([C:5]2[C:7]3[C:8](=[CH:12][C:13]([O:16][CH3:17])=[CH:14][CH:15]=3)[C:9](=[O:10])[NH:24][N:23]=2)[CH:18]=[CH:19][C:20]=1[CH3:21]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 692132722-(3,4-Dimethylbenzoyl)-5-methoxybenzoic acid

Product 1

HCID 692123094-(3,4-dimethylphenyl)-7-methoxy-2H-phthalazin-1-one

Procedure

This compound is obtained according to the procedure described in 1.2. by reacting 2-(3,4-dimethylbenzoyl)-5-methoxybenzoic acid with hydrazine hydrate.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-9caaebfb4bed4abe9a4484727fddbd85
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

Loading…