Hydrazine hydrate (1:1) → 7-Methoxy-4-phenoxymethyl-2h-phthalazin-1-one

HRID 30042Notes

Reaction equation

HRID 30042 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:12](=O)[CH2:13][O:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[C:7]([CH:11]=1)[C:8](O)=[O:9].O.[NH2:23][NH2:24]>>[CH3:1][O:2][C:3]1[CH:11]=[C:7]2[C:6]([C:12]([CH2:13][O:14][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[N:23][NH:24][C:8]2=[O:9])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 692132605-Methoxy-2-(2-phenoxyacetyl)benzoic acid

Product 1

HCID 692122937-Methoxy-4-phenoxymethyl-2h-phthalazin-1-one

Procedure

This compound is obtained according to the procedure described in 1.2. by reacting 5-methoxy-2-(2-phenoxyacetyl)benzoic acid with hydrazine hydrate.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-0c9ea9c04dda4acdb8100ddab16a0523
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

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