Hydrazine hydrate (1:1) → 7-methoxy-5-phenyl-2H-phthalazin-1-one
Reaction equation
[CH:1]([C:3]1[C:11]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:10][C:9]([O:18][CH3:19])=[CH:8][C:4]=1[C:5](O)=[O:6])=O.O.[NH2:21][NH2:22]>>[CH3:19][O:18][C:9]1[CH:8]=[C:4]2[C:3]([CH:1]=[N:21][NH:22][C:5]2=[O:6])=[C:11]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:10]=1Participants
3
Procedure
This compound is obtained according to the procedure described in 1.2. by reacting 2-formyl-5-methoxy-3-phenylbenzoic acid with hydrazine hydrate.
Workup
- customThis compound is obtained
Sources & evidence
- ORD record
- ord-b44f67aab3764d7c9c5ce9565ad90598
- Source dataset
- uspto-grants-2008_09
- Patent number
- US07423030B2
Reaction notes
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