Hydrazine hydrate (1:1) → 4-benzyloxymethyl-7-methoxy-2H-phthalazin-1-one

HRID 30059Notes

Reaction equation

HRID 30059 reaction equation
[CH2:1]([O:8][CH2:9][C:10]([C:12]1[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][C:13]=1[C:14](O)=[O:15])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.O.[NH2:24][NH2:25]>>[CH2:1]([O:8][CH2:9][C:10]1[C:12]2[C:13](=[CH:17][C:18]([O:21][CH3:22])=[CH:19][CH:20]=2)[C:14](=[O:15])[NH:25][N:24]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 69212695HCID 69212695, compound

Product 1

HCID 692108214-benzyloxymethyl-7-methoxy-2H-phthalazin-1-one

Procedure

This compound is obtained according to the procedure described in 1.2. by reacting 2-(2-benzyloxyacetyl)-5-methoxybenzoic acid with hydrazine hydrate.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-3567efeb3dc444caa2a39d2c8df2fafe
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

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