Phosphorus oxychloride → HCID 86612237, compound

HRID 30060Notes

Reaction equation

HRID 30060 reaction equation
[CH2:1]([O:8][CH2:9][C:10]1[C:19]2[C:14](=[CH:15][C:16]([O:20][CH3:21])=[CH:17][CH:18]=2)[C:13](=O)[NH:12][N:11]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.P(Cl)(Cl)([Cl:25])=O>>[CH2:1]([O:8][CH2:9][C:10]1[C:19]2[C:14](=[CH:15][C:16]([O:20][CH3:21])=[CH:17][CH:18]=2)[C:13]([Cl:25])=[N:12][N:11]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 692108214-benzyloxymethyl-7-methoxy-2H-phthalazin-1-one

Product 1

HCID 86612237HCID 86612237, compound

Procedure

This compound is obtained according to the procedure described in 1.3. by reacting 4-benzyloxymethyl-7-methoxy-2H-phthalazin-1-one with phosphoryl chloride. This oily compound is used as obtained in the following reaction.

Workup

  1. customThis compound is obtained
  2. customas obtained in the following reaction

Sources & evidence

ORD record
ord-b5b0ae5efff54c58a887f972efb5f06e
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

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