Hydrochloric Acid → HCID 59789454, compound

HRID 30238Notes

Reaction equation

HRID 30238 reaction equation
Cl.C(OC([N:9]1[CH2:22][CH:12]2[C:13]3[C:14]([C:20]#[N:21])=[C:15]([Cl:19])[S:16][C:17]=3[CH2:18][CH:11]2[CH2:10]1)=O)(C)(C)C>>[Cl:19][C:15]1[S:16][C:17]2[CH2:18][CH:11]3[CH2:10][NH:9][CH2:22][CH:12]3[C:13]=2[C:14]=1[C:20]#[N:21]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 131727021HCID 131727021, compound

Product 1

HCID 59789454HCID 59789454, compound

Procedure

The title compound was prepared as its HCl salt by the method of Example 1, step b) utilizing the product of step d). 1H NMR (300 MHz, CDCl3, ppm) 2.75-2.82 (m, 1H); 2.92-3.05 (m, 1H); 3.12-3.45 (m, 4H); 3.50-3.62 (m, 1H); 3.82-3.95 (m, 1H); 7.10-7.30 (br s, 2H); MS calculated for C10H9ClN2S+H 225, observed 225.

Sources & evidence

ORD record
ord-18bb9bf0c728480b96dbd8b56823dd0e
Source dataset
uspto-grants-2008_09
Patent number
US07423056B2

Reaction notes

Loading…