HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 11651418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 131727024 | HCID 131727024 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11651418 | HCID 11651418 | — |
Reaction Steps
The product of step d) was treated with 40% aqueous KOH in EtOH at 105° C. for 16 hours. The reaction was cooled, diluted with CH2Cl2 and passed through an extrelut column to remove the water. The organic layer was concentrated and the residue purified by preparative LC/MS to give the title compound. MS calculated for C10H12ClNS+H 214, observed 214.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423056B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-42e4da9170d742b8a5b27248ef620543 |
| Source note | uspto-grants-2008_09 |