HCID 58624931, compound → HCID 67206869, compound

HRID 30257Notes

Reaction equation

HRID 30257 reaction equation
C[O:2][C:3]([CH:5]1[CH:9]([C:10]2[S:11][CH:12]=[C:13]([Br:15])[CH:14]=2)[CH2:8][N:7]([CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:6]1)=[O:4]>Cl>[CH2:16]([N:7]1[CH2:8][CH:9]([C:10]2[S:11][CH:12]=[C:13]([Br:15])[CH:14]=2)[CH:5]([C:3]([OH:4])=[O:2])[CH2:6]1)[C:17]1[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1

Participants

3

Reactant 1

HCID 58624931HCID 58624931, compound

Product 1

HCID 67206869HCID 67206869, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Conditions

Temperature
85 °C

Procedure

The product of step b) (4.3 g, 11.3 mmol) was dissolved in 6M HCl and stirred at 85° C. for 16 hours. Next, the solvent was evaporated in vacuo providing the subtitle compound that was used without further purification. MS calculated for C16H16BrNO2S−H 364, observed 364, 366.

Workup

  1. customNext, the solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-3eefdcc94dbf4baeae0889751e210ea8
Source dataset
uspto-grants-2008_09
Patent number
US07423056B2

Reaction notes

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