HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Bromo-thiophen-2-yl)-1-(1-phenyl-ethyl)-pyrrolidine-3-carboxylic acid methyl ester → HCID 67317858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Bromo-thiophen-2-yl)-1-(1-phenyl-ethyl)-pyrrolidine-3-carboxylic acid methyl ester | HCID 67204896 | — |
| Reactant | 1,2,3,3a,7,7a-Hexahydro-4-thia-2-aza-cyclopenta[alpha]pentalene-6-carbonitrile | HCID 68301759 | — |
| Product | HCID 67317858 | HCID 67317858 | 100% |
Reaction Steps
The product of step b), diastereomer 1 (15 g, 0.038 mol) was treated by the method outlined in Example 34, step c) to afford the subtitle compound (14.7 g, yield: 100%). MS calculated for C17H18BrNO2S+H: 380, observed 380 and 383.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423056B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-838da65c46e447e785cac488f6d87328 |
| Source note | uspto-grants-2008_09 |