HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86601065, compound → HCID 86601064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86601065 | HCID 86601065 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86601064 | HCID 86601064 | 73% |
Reaction Steps
The title compound was prepared according to the general method of Example 14 (c) except that dilute acetic acid was used for neutralization of the reaction mixture. The desired product (0.83 g, 73%) was prepared as a yellow solid starting from 6-amino-1-(4-methoxybenzyl)-5-nitroso-2-thioxo-2,3-dihydro-1H-pyrimidin-4-one (1.2 g, 4.1 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425560B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-cbc0049e41334b26aa1b0f09e69672b6 |
| Source note | uspto-grants-2008_09 |