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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 31072Generated: October 29, 2026

HCID 86601065, compound → HCID 86601064, compound

https://huagongshe.com/reaction/31072

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86601065HCID 86601065—
SolventAcetic AcidHCID 176—
ProductHCID 86601064HCID 8660106473%

Reaction Steps

The title compound was prepared according to the general method of Example 14 (c) except that dilute acetic acid was used for neutralization of the reaction mixture. The desired product (0.83 g, 73%) was prepared as a yellow solid starting from 6-amino-1-(4-methoxybenzyl)-5-nitroso-2-thioxo-2,3-dihydro-1H-pyrimidin-4-one (1.2 g, 4.1 mmol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07425560B2
Source datasetuspto-grants-2008_09
ORD IDord-cbc0049e41334b26aa1b0f09e69672b6
Source noteuspto-grants-2008_09