HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 11254099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 15520870 | HCID 15520870 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11254099 | HCID 11254099 | — |
Reaction Steps
1.8 g (8.14 mmol) of 5-[1-(pyrrolidin-1-yl-carbonyl)-cyclopropyl]-2-chloro-nitrobenzene are dissolved in 30 ml of ethyl acetate and 30 ml of ethanol and after the addition of 0.8 g palladium on active charcoal (10%) hydrogenated for 3 hours at ambient temperature with hydrogen. Then the catalyst is filtered off and the filtrate is evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425641B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-9fc8f498ad224429bd573b1a57ac66fb |
| Source note | uspto-grants-2008_09 |