HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(Piperazine-1-sulfonyl)morpholine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69273755 | HCID 69273755 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-(Piperazine-1-sulfonyl)morpholine hydrochloride | HCID 42883596 | — |
Reaction Steps
4-(Morpholine-4-sulfonyl)-piperazine-1-carboxylic acid tert-butyl ester (39 mg) was dissolved in 4 mL of dioxane, and 4 mL of 4.0 M hydrochloric acid in dioxane was added. After standing overnight at ambient temperature, the solvent was removed to give 4-(piperazine-1-sulfonyl)-morpholine hydrochloride as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425638B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-c72c463ce5b74f8b83f67fa8a8cd7319 |
| Source note | uspto-grants-2008_09 |