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HRID31511

反应详情

EQUATION

反应方程式

HRID 31511 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)N1CCN(S(=O)(=O)N2CCOCC2)CC1
HCID69273755

未命名化合物

PRODUCTS

生成物

1
结构：Cl.O=S(=O)(N1CCNCC1)N1CCOCC1
HCID42883596

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

2 次

PROCEDURE

实验过程

4-(Morpholine-4-sulfonyl)-piperazine-1-carboxylic acid tert-butyl ester (39 mg) was dissolved in 4 mL of dioxane, and 4 mL of 4.0 M hydrochloric acid in dioxane was added. After standing overnight at ambient temperature, the solvent was removed to give 4-(piperazine-1-sulfonyl)-morpholine hydrochloride as a white solid.

WORKUP

后处理

  1. customthe solvent was removed