HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → 2-(2-Methyl-1,3-dioxan-2-yl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | 2-(2-Propyl-1,3-dioxan-2-yl)ethanol | HCID 59792435 | — |
| Product | 2-(2-Methyl-1,3-dioxan-2-yl)ethanol | HCID 59656768 | 49% |
Reaction Steps
The same procedure as in the steps (8a) and (8b) of Example 8, was repeated using ethyl acetoacetate to obtain the title compound (5.4 g, total yield: 49%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425634B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-f1c96fd3e135466e981fd004cf3af29f |
| Source note | uspto-grants-2008_09 |