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HRID31663

反应详情

EQUATION

反应方程式

HRID 31663 的结构方程式

REACTANTS

反应物

3
结构：Cc1c(Cl)cc[n+]([O-])c1C
HCID9877446

4-Chloro-2,3-dimethyl-1-oxo-1lambda~5~-pyridine

C7H8ClNO

结构：COCC1(CCO)OCCO1
HCID59792568

未命名化合物

结构：Cc1c(OCC2(C)OCC3(CO2)OCCO3)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66776550

未命名化合物

PRODUCTS

生成物

1
结构：COCC1(CCOc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)OCCO1.[Na]
HCID66776626

未命名化合物

收率 3.9%

PROCEDURE

实验过程

The same procedure as in the steps (5d) to (5h) of Example 5 was repeated using 4-chloro-2,3-dimethylpyridine 1-oxide and 2-(2-(methoxymethyl)-1,3-dioxolan-2-yl)ethanol to obtain the title compound (312 mg, 5 steps 3.9%) as a light yellow foam.