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HRID31716

反应详情

EQUATION

反应方程式

HRID 31716 的结构方程式

REACTANTS

反应物

3
结构：COC1OCC(COc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)CO1
HCID12003120

未命名化合物

结构：CCc1c(OCC2COC(C)(C)OC2)ccnc1CO
HCID59792593

未命名化合物

结构：COC1OCC(COc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)CO1.[Na]
HCID66776002

未命名化合物

PRODUCTS

生成物

1
结构：CCc1c(OCC2COC(C)(C)OC2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66775723

未命名化合物

收率 25%

PROCEDURE

实验过程

The same procedure as in the steps (6d), (6e), and (6f) of Example 6 was repeated using the (4-((2,2-dimethyl-1,3-dioxan-5-yl)methoxy)-3-ethylpyridin-2-yl)methanol obtained in the step (92d) above to obtain the title compound (159 mg, overall yield: 25%) as a light yellow solid.

WORKUP

后处理

  1. customobtained in the step (92d) above