HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 9869065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 15521930 | HCID 15521930 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 9869065 | HCID 9869065 | — |
Reaction Steps
To a solution of 4-12 (0.20 g, 0.41 mmol) in EtOH (5 mL) was added 1N NaOH (0.5 ml, 0.5 mmol). After stirring for 2 h, the solvents were evaporated and the residue was chromatographed (silica gel, 25:10:1:1 followed by 15:10:1:1 ethyl acetate/EtOH/water/NH4OH) to give 4-13 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211191B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f2c42c72a6d14067b061bdc5326f5ec9 |
| Source note | uspto-grants-2001_04 |