HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 13079701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 3-[4-(Benzyloxy)phenyl]propan-1-ol | HCID 2764076 | — |
| Product | HCID 13079701 | HCID 13079701 | 98% |
Reaction Steps
In substantially the same manner as in Reference Example 12, 3-(4-benzyloxyphenyl)propanol was allowed to react with methanesulfonyl chloride to give 3-(4-benzyloxyphenyl)propyl methanesulfonate. The yield was 98%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 74-75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-d59ab3bf40164379b203e3c0417672ed |
| Source note | uspto-grants-2001_04 |