HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloroacetone → HCID 22009760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | 9-fluorenylideneacetamide | HCID 297944 | — |
| Product | HCID 22009760 | HCID 22009760 | 36% |
Reaction Steps
In substantially the same manner as in Reference Example 47, 9-fluorenylideneacetamide was allowed to react with 1,3-dichloroacetone to give 4-chloromethyl-2-(9-fluorenylidene)methyloxazole. The yield was 36%. Recrystallization from ethyl acetate-hexane gave yellow prisms, mp 175-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-a3c83f046d934ddb954e5e4a6a2c079f |
| Source note | uspto-grants-2001_04 |