HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloroacetone → HCID 22009778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | HCID 22009589 | HCID 22009589 | — |
| Product | HCID 22009778 | HCID 22009778 | 65% |
Reaction Steps
In substantially the same manner as in Reference Example 47, 2-phenyl-5-benzoxazolecarboxamide was allowed to react with 1,3-dichloroacetone to give 5-(4-chloromethyl-2-oxazolyl)-2-phenylbenzoxazole. The yield was 65%. Recrystallization from ethyl acetate-hexane gave brown needles, mp 194-195° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-cf2d7897aa964d00a9bb63a6ac35e277 |
| Source note | uspto-grants-2001_04 |