HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → 1-[3-(3-Benzyloxyphenyl)propyl]imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | 3-(3-Benzyloxyphenyl)propyl methanesulfonate | HCID 22733363 | — |
| Product | 1-[3-(3-Benzyloxyphenyl)propyl]imidazole | HCID 22009713 | 44% |
Reaction Steps
In substantially the same manner as in Reference Example 88, 3-(3-benzyloxyphenyl)propyl methanesulfonate was allowed to react with imidazole to give 1-[3-(3-benzyloxyphenyl)propyl]imidazole. The yield was 44%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 82-83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-1002c7a0a09a4c3593c1499cc7232107 |
| Source note | uspto-grants-2001_04 |