HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2728534, compound → HCID 22009757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2728534 | HCID 2728534 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 22009757 | HCID 22009757 | 69% |
Reaction Steps
In substantially the same manner as in Reference Example 77, ethyl 2-(1-pyrrolyl)-4-thiazolecarboxylate was reduced by lithium aluminum hydride to give 2-(1-pyrrolyl)-4-thiazolylmethanol. The yield was 69%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 111-113° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-902439555ada4fe4b2b7f9b664e7ed61 |
| Source note | uspto-grants-2001_04 |