HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22009685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 22009825 | HCID 22009825 | — |
| Product | HCID 22009685 | HCID 22009685 | 74% |
Reaction Steps
In substantially the same manner as in Reference Example 111, ethyl 5-(2-thienyl)-2-thiazolecarboxylate was subjected to reduction with sodium borohydride to obtain 5-(2-thienyl)-2-thiazolylmethanol. The yield was 74%. Recrystallization from ethyl acetate-hexane gave pale yellow prisms, mp 67-68° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-167d7164fea04a78a644b5f25dccaafe |
| Source note | uspto-grants-2001_04 |