HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18673021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Ethyl 2-(2-thienyl)-5-thiazolecarboxylate | HCID 22009660 | — |
| Product | HCID 18673021 | HCID 18673021 | 94% |
Reaction Steps
In substantially the same manner as in Reference Example 111, ethyl 2-(2-thienyl)-5-thiazolecarboxylate was subjected to reduction with sodium borohydride to obtain 2-(2-thienyl)-5-thiazolylmethanol. The yield was 94%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 89-90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-76174db9c9b2470cb97e1e3ad0d087ff |
| Source note | uspto-grants-2001_04 |