HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22009767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22009730 | HCID 22009730 | — |
| Product | HCID 22009767 | HCID 22009767 | 96% |
Reaction Steps
In substantially the same manner as in Reference Example 73, 7-phenyl-3-quinolylmethanol was reacted with thionyl chloride to obtain 3-chloromethyl-7-phenylquinoline. The yield was 96%. Recrystallization from ethyl acetate-hexane gave colorless prisms, 105-106° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-098f26b6880d466f9efbd16490ac8996 |
| Source note | uspto-grants-2001_04 |