HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22009689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22009839 | HCID 22009839 | — |
| Product | HCID 22009689 | HCID 22009689 | 77% |
Reaction Steps
In substantially the same manner as in Reference Example 73, 7-(2-thienyl)-3-quinolylmethanol was reacted with thionyl chloride to obtain 3-chloromethyl-7-(2-thienyl)quinoline. The yield was 77%. Recrystallization from ethyl acetate-hexane gave colorless leaflets, 120-121° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-8f32e36694cd49cfa18f2108268e035e |
| Source note | uspto-grants-2001_04 |