HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4065946, compound → 3-[4-(Benzyloxy)-3-methoxyphenyl]propan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4065946 | HCID 4065946 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 3-[4-(Benzyloxy)-3-methoxyphenyl]propan-1-ol | HCID 14520853 | 56% |
Reaction Steps
In substantially the same manner as in Reference Example 82, ethyl 4-benzyloxy-3-methoxycinnamate was subjected to reduction with lithium aluminum hydride to obtain 3-(4-benzyloxy-3-methoxyphenyl)propanol. The yield was 56%. Recrystallization from ethyl acetate-hexane gave colorless prisms, 57-58° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-63bf6bfc321c44ce81df430c711d3926 |
| Source note | uspto-grants-2001_04 |