HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 3-(3-Chloro-4-methoxymethoxyphenyl)propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | Ethyl 3-(3-chloro-4-methoxymethoxyphenyl)propionate | HCID 22009674 | — |
| Product | 3-(3-Chloro-4-methoxymethoxyphenyl)propanol | HCID 22009614 | 97% |
Reaction Steps
In substantially the same manner as in Reference Example 82, ethyl 3-(3-chloro-4-methoxymethoxyphenyl)propionate was subjected to reduction with lithium aluminum hydride to obtain 3-(3-chloro-4-methoxymethoxyphenyl)propanol as an oil. The yield was 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-7eb7a663804f46d8b3cc3fa07f3cfc0e |
| Source note | uspto-grants-2001_04 |